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 | Acesso ao texto completo restrito à biblioteca da Embrapa Agroindústria de Alimentos. Para informações adicionais entre em contato com ctaa.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Agroindústria de Alimentos. |
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Data corrente: |
03/10/2017 |
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Data da última atualização: |
14/03/2019 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
MIRANDA, J. A. T. de; CARVALHO, L. M. J. de; CASTRO, I. M. de; VIERA, A. C. de M.; FIGUEIREDO, V. de O.; ANJOS, M. R. dos; DELLA MORA ORTIZ, G. M. |
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Afiliação: |
Joyce Aparecida Tavares de Miranda, UFRJ; Lucia Maria Jaeger de Carvalho, UFRJ; IZABELA MIRANDA DE CASTRO, CTAA; Ana Cláudia de Macêdo Vieira, UFRJ; Verônica de Oliveira Figueiredo, UFRJ; MARIANNA RAMOS DOS ANJOS, CTAA; Gisela Maria Dellamora Ortiz, UFRJ. |
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Título: |
Validation of a method for determination of organophosphates in black bean samples. |
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Ano de publicação: |
2017 |
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Fonte/Imprenta: |
International Journal of Current Research, v. 9, n. 3, p. 48261-48263, march, 2017. |
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Idioma: |
Inglês |
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Conteúdo: |
The presence of pesticides residues above the Acceptable Daily Intake values and the Maximum Residue Limits is worrying in the point of view of food safety. In order to identify and determine the presence of organ phosphorus pesticides in bean samples, a multiresidue technique of extraction a multiresidue technique of extraction method was applied, and the analyses were conducted by gas chromatography coupled to a thermoionic flame detector (GC-FTD). This study aimed to validate the methodology of etermination of organophosphates by studies of selectivity, linearity, intermediate precision, limit of detection, limit of quantification, and accuracy study by addition and recovery. The method was selective for all analytes, because there was no interference higher than 30% of the limit of quantification. The limits of detection were between 1.60 and 52.96 ng.kg-1 and the quantification limits were between 3.30 and 176.0 ng.kg-1. Regarding intermediate precision, the differences of area values were ? 15%, in different concentrations, except for phorate. The correlation coefficients (r) of linearity curves were higher than 0.99 for all active ingredients, within the working range applied. The recovery percentage was between 70 and 120%, except for phorate. Thus, the methodology was satisfactory for identification and determination of ten from the eleven organophosphates analyzed in beans. |
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Palavras-Chave: |
Bean; Organophosphorus; Validation. |
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Categoria do assunto: |
-- |
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Marc: |
LEADER 02123naa a2200229 a 4500
001 2076624
005 2019-03-14
008 2017 bl uuuu u00u1 u #d
100 1 $aMIRANDA, J. A. T. de
245 $aValidation of a method for determination of organophosphates in black bean samples.$h[electronic resource]
260 $c2017
520 $aThe presence of pesticides residues above the Acceptable Daily Intake values and the Maximum Residue Limits is worrying in the point of view of food safety. In order to identify and determine the presence of organ phosphorus pesticides in bean samples, a multiresidue technique of extraction a multiresidue technique of extraction method was applied, and the analyses were conducted by gas chromatography coupled to a thermoionic flame detector (GC-FTD). This study aimed to validate the methodology of etermination of organophosphates by studies of selectivity, linearity, intermediate precision, limit of detection, limit of quantification, and accuracy study by addition and recovery. The method was selective for all analytes, because there was no interference higher than 30% of the limit of quantification. The limits of detection were between 1.60 and 52.96 ng.kg-1 and the quantification limits were between 3.30 and 176.0 ng.kg-1. Regarding intermediate precision, the differences of area values were ? 15%, in different concentrations, except for phorate. The correlation coefficients (r) of linearity curves were higher than 0.99 for all active ingredients, within the working range applied. The recovery percentage was between 70 and 120%, except for phorate. Thus, the methodology was satisfactory for identification and determination of ten from the eleven organophosphates analyzed in beans.
653 $aBean
653 $aOrganophosphorus
653 $aValidation
700 1 $aCARVALHO, L. M. J. de
700 1 $aCASTRO, I. M. de
700 1 $aVIERA, A. C. de M.
700 1 $aFIGUEIREDO, V. de O.
700 1 $aANJOS, M. R. dos
700 1 $aDELLA MORA ORTIZ, G. M.
773 $tInternational Journal of Current Research$gv. 9, n. 3, p. 48261-48263, march, 2017.
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Registro original: |
Embrapa Agroindústria de Alimentos (CTAA) |
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| Registros recuperados : 14 | |
| 3. |  | MIRANDA, J. A. T.; CARVALHO, L. M. J.; CASTRO, I. M. de; FIGUEIREDO, V.; TEIXEIRA, A. S.; ANJOS, M. R. Influence of heat treatment on the degradation of organophosphates in cooked beans (Phaseolus vulgaris). In: LATIN AMERICAN PESTICIDE RESIDUE WORKSHOP FOOD AND ENVIROMENT, 5., 2015, Santiago, Chile. Book of abstracts... Santiago: Pontificia Universidad Católica de Chile, 2015. 1 CD-ROM. p. 245. In: LATIN AMERICAN PESTICIDE RESIDUE WORKSHOP, 5., 2015, Santiago, Chile. Food and enviroment. Santiago: Pontificia Universidad Católica de Chile, 2015. 1 CD-ROM. LAPRW 2015. Cód. PO10.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 5. | | MIRANDA, J. A. T.; FOGACA, F. H. dos S.; CUNHA, S. C.; ALONSO, M. B.; TORRES, J. P.; FERNANDES, J. O. Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil. International Journal of Environmental Research and Public Health, v. 19, 15790, p. 1-14, 2022.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 1 |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
|  |
| 7. | | MIRANDA, J. A. T. de; CUNHA, S. C.; FOGACA, F. H. dos S.; ALONSO, M. B.; TORRES, J. P. M.; MARQUES, A.; FERNANDES, J. O. Otimização de um método de extração de multiresíduos para análise de pesticidas. In: ENCONTRO BRASILEIRO DE DESREGULADORES ENDÓCRINOS, 2; SIMPÓSIO DE ATUALIZAÇÃO DE DESREGULADORES ENDÓCRINOS, 3. 2020, UFRJ. 17 A 20 de novembro de 2020.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 9. | | CARVALHO, L. M. J. de; FIGUEIREDO, V. O.; CASTRO, I. M. de; MIRANDA, J. A. T.; COLARES, L. G. T.; CARVALHO, J. L. V. de. Organophosphorus pesticides residues in cooked tomato (Licopersicum esculentum). In: WORLD CONGRESS OF FOOD SCIENCE AND TECHNOLOGY & EXPO, 17., 2014, Montreal. Book of abstracts. [S.l.]: IUFoST, 2014. Ref. UP272.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 10. | | MIRANDA, J. A. T. DE; CARVALHO, L. M. J. DE; CASTRO, I. M. de; ANJOS, M. R. dos; CARVALHO, J. L. V. de; VIEIRA, A. C. DE M. Heating, Identification, and Determination of Pesticides Residues in Black Bean Samples. Chemical Engineering Transactions, v. 80, 2020. p. 337-342| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 2 |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 11. | | CUNHA, S. C.; MENEZES-SOUSA, D.; MELLO, F. V.; MIRANDA, J. A. T.; FOGACA, F. H. dos S.; ALONSO, M. B.; TORRES, J. P. M.; FERNADES, J. O. Survey on endocrine-disrupting chemicals in seafood: Occurrence and distribution. Environmental Research, v. 210, 112886, 2022.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 1 |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 12. | | CARVALHO, L. M. J.; GUIMARÃES, A.; VIEIRA, A. C. M.; MIRANDA, J. A. T.; BARBOSA, D. M. C.; CARVALHO, J. L. V. de; ALBUQUERQUE, I.; ANTUNES, E. R.; TAVARES, C. P. Evaluation of (C. moschata) pumpkin in natura by optic microscopy. In: EUROPEAN FEDERATION OF FOOD SCIENCE AND TECHNOLOGY CONFERENCE, 31., Spain. Food Science and Technology Challenges for the 21st Century - Research to Progress Society. Spain: EFFoST, 2017. P1.032.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 13. | | MIRANDA, J. A. T. de; CARVALHO, L. M. J. de; CASTRO, I. M. de; VIERA, A. C. de M.; FIGUEIREDO, V. de O.; ANJOS, M. R. dos; DELLA MORA ORTIZ, G. M. Validation of a method for determination of organophosphates in black bean samples. International Journal of Current Research, v. 9, n. 3, p. 48261-48263, march, 2017.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: B - 3 |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 14. | | MIRANDA, J. A. T. DE; CARVALHO, L. M. J. DE; CASTRO, I. M. de; CARVALHO, J. L. V. de; GUIMARÃES, A. L. DE A.; VIEIRA, A. C. DE M. Starch granules from cowpea, black, and carioca beans in raw and cooked forms. In: EL-ESAWI, M. A. (Ed.). Legume Crops: Characterization and Breeding for Improved Food Security. [s.l.]: IntechOpen, 2019. Disponível em: . Acesso em: 02 dez. 2019. 20 p.| Tipo: Capítulo em Livro Técnico-Científico |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| Registros recuperados : 14 | |
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| Nenhum registro encontrado para a expressão de busca informada. |
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